Hydroxypropyl cellulose grafted with poly （butyl methacrylate）

GUO Ming; SONG Chuan-hu; LU Di; WANG Huan; Li-ping

doi:10.11833/j.issn.2095-0756.2011.01.021

Volume 28 Issue 1

Feb. 2011

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GUO Ming, SONG Chuan-hu, LU Di, WANG Huan, Li-ping. Hydroxypropyl cellulose grafted with poly （butyl methacrylate）[J]. Journal of Zhejiang A&F University, 2011, 28(1): 132-138. doi: 10.11833/j.issn.2095-0756.2011.01.021

Citation:

GUO Ming, SONG Chuan-hu, LU Di, WANG Huan, Li-ping. Hydroxypropyl cellulose grafted with poly （butyl methacrylate）[J]. Journal of Zhejiang A&F University, 2011, 28(1): 132-138. doi: 10.11833/j.issn.2095-0756.2011.01.021

Hydroxypropyl cellulose grafted with poly （butyl methacrylate）

doi: 10.11833/j.issn.2095-0756.2011.01.021

1.
School of Sciences，Zhejiang A & F University，Lin’an 311300，Zhejiang，China

More Information

Corresponding author: GUO Ming
Publish Date: 2011-02-20

Abstract

Hydroxypropyl cellulose （HPC） grafted with poly（butyl methacrylate）（PBMA） copolymer （HPC-g-PBMA）was synthesized using emulsion copolymerization of the HPC monomer and butyl methacrylate （BMA）. Structure of the grafted copolymer was described with Fourier transform-infrared （FT-IR） spectroscopy，X-ray diffraction （XRD） analysis，and scanning electronic microscope （SEM）. Thermogravimetric analysis （TGA） and differential scanning calorimetry（DSC） were used to analyze thermodynamic properties，and solubility was also tested. Optimum synthetic conditions for HPC-g-PBMA were determined through an orthogonal experiment. Results indicated that the structure of HPC-g-PBMA differed from HPC with thermoplasticity of the graft copolymer improved . Due to a superior resistance to strong acids，strong base and organic solvent was obtained. ［Ch，9 fig. 7 tab. 18 ref.］
- hydroxypropyl cellulose（HPC）,
- butyl methacrylate,
- graft copolymerization,
- structural characterization

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通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

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Hydroxypropyl cellulose grafted with poly （butyl methacrylate）

1. School of Sciences，Zhejiang A & F University，Lin’an 311300，Zhejiang，China

Corresponding author: GUO Ming

Publish Date: 2011-02-20

Key words:

Abstract: Hydroxypropyl cellulose （HPC） grafted with poly（butyl methacrylate）（PBMA） copolymer （HPC-g-PBMA）was synthesized using emulsion copolymerization of the HPC monomer and butyl methacrylate （BMA）. Structure of the grafted copolymer was described with Fourier transform-infrared （FT-IR） spectroscopy，X-ray diffraction （XRD） analysis，and scanning electronic microscope （SEM）. Thermogravimetric analysis （TGA） and differential scanning calorimetry（DSC） were used to analyze thermodynamic properties，and solubility was also tested. Optimum synthetic conditions for HPC-g-PBMA were determined through an orthogonal experiment. Results indicated that the structure of HPC-g-PBMA differed from HPC with thermoplasticity of the graft copolymer improved . Due to a superior resistance to strong acids，strong base and organic solvent was obtained. ［Ch，9 fig. 7 tab. 18 ref.］

Hydroxypropyl cellulose grafted with poly （butyl methacrylate）

doi: 10.11833/j.issn.2095-0756.2011.01.021

Abstract

References

Proportional views

通讯作者: 陈斌, bchen63@163.com

Related

Proportional views